https://doi.org/10.1351/goldbook.08414
Solid-state nuclear magnetic resonance spectroscopy on a single crystal in a similar manner to that used in X-ray diffraction.
Note:
A large crystal is mounted on a 'tenon', which is in turn mounted on a goniometer head. If the orientation of the unit cell is known with respect to the tenon, then it is possible to determine the orientation of the NMR interaction tensors with respect to the molecular frame.
A large crystal is mounted on a 'tenon', which is in turn mounted on a goniometer head. If the orientation of the unit cell is known with respect to the tenon, then it is possible to determine the orientation of the NMR interaction tensors with respect to the molecular frame.